The optimization of solid phase micro-extraction conditions for volatile compounds of Camellia oil

Long Qi zhi, Huang Yong-hui, Zhong Hai-yan, Long Zhonghai, Paul Prenzler, Kevin Robards

Research output: Contribution to journalArticle

Abstract

Volatile extraction of camellia oil (Camellia oleifera Abel) by headspace solid phase microextraction-gaschromatography (HS-SPME-GC) using 50/30 'm DVB/CAR/PDMS fiber are presented. Parameters such as total peak area, ratio of total peak area to number of peaks, peak number and peak area of main volatiles were used for optimization of extraction variables. Extraction conditions that gave good total recovery and diversity of compounds from camellia oil headspace were found to be: 1 g oil sample in 15 mL vessel; exposure for 25 min at40 '; stirring at 100 r/min and desorption for 3 min at 260 '.
Original languageEnglish
Pages (from-to)70-74
Number of pages5
JournalJournal of the Chinese Cereals and Oils Association
Volume24
Issue number1
Publication statusPublished - 2009

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